Sample Submission
Anytime in room -1.117 or appointment with the instrument's contact person.

Sample Amount
¹H,¹⁹F,³¹P: > 1 mM (corresponds to 0.1 mg for MW = 160)
COSY/NOESY/DOSY/HSQC/HMBC: > 10 mM (corresponds to 1 mg for MW = 160)
¹³C,¹⁵N-HMBC,²⁹Si: > 100 mM (corresponds to 10 mg for MW = 160)
further nuclei: depending on their sensitivity

Solvents
Use deuterated solvents only!
We have several less common solvents (diethyl ether, pyridine...) in stock.
Upon request we can do the sample preparation.

Filling Height
40–50 mm (corresponds to 550-700 uL) !!

Sample Quality
Completely dissolved, clear and homogeneous solutions. Please make sure the tubes are clean, undamaged und tightly sealed.

Tube Length
At least 7 inch

Service Measurement Form (see below)
Please fill in completely and readible and put the form into the box on the desk. The first 2-3 characters in the field "filename" should indentify the "customer". Please use the same code as in "filename" for labelling the tube and deposit the sample in the refridgerator.

NMR Data
After the measurement all data files are copied to the server under the name "filename" plus a code identifying the instrument and experiment (e.g. 3h für ¹H 300 MHz). Also a plot of the full spectrum is provided in room -1.117.